{"created":"2023-06-20T15:17:12.816261+00:00","id":47365,"links":{},"metadata":{"_buckets":{"deposit":"9410ebde-1919-440b-9770-20ab13bfdf21"},"_deposit":{"created_by":1,"id":"47365","owners":[1],"pid":{"revision_id":0,"type":"depid","value":"47365"},"status":"published"},"_oai":{"id":"oai:jaxa.repo.nii.ac.jp:00047365","sets":["1398:1421:2114","1887:1893","9:10:2065:2113"]},"author_link":["532440","532443","532439","532438","532442","532441"],"item_3_alternative_title_2":{"attribute_name":"その他のタイトル（英）","attribute_value_mlt":[{"subitem_alternative_title":"Study on Thermal Decomposition Characteristic of FOX-12 based on Thermal Analysis with in-situ Observation and Spectroscopic Analysis"}]},"item_3_biblio_info_10":{"attribute_name":"書誌情報","attribute_value_mlt":[{"bibliographicIssueDates":{"bibliographicIssueDate":"2021-02-10","bibliographicIssueDateType":"Issued"},"bibliographicPageEnd":"25","bibliographicPageStart":"22","bibliographicVolumeNumber":"JAXA-RR-20-007","bibliographic_titles":[{"bibliographic_title":"宇宙航空研究開発機構研究開発報告: 高エネルギー物質研究会: 令和2年度研究成果報告書"},{"bibliographic_title":"JAXA Research and Development Report: Technical Report of The Research Activity for High Energy Materials (2020)","bibliographic_titleLang":"en"}]}]},"item_3_description_17":{"attribute_name":"抄録（英）","attribute_value_mlt":[{"subitem_description":"Guanylurea dinitramide which is usually called FOX-12 is typical dinitramide salts. To obtain better understanding of thermal decomposition characteristic of FOX-12, this paper focused on analysis of initial decomposition of FOX-12 using in situ measurement with differential scanning calorimetry (DSC) and sample observation or Raman spectrometry for understanding decomposition characteristic of FOX-12. We conducted Raman spectroscopic analysis and sample observation during thermal analysis at 1 and 8 C min-1. The experiment results found that thermal behavior of FOX-12 was different by heating rate and formed condensed phase before sharp exotherm at high heating rate. For DSC/Raman result indicated guanidium nitrate (GN) and cyanuric acid formed during thermal decomposition of FOX-12. From observation results, GN and cyanuric acid formed with solid phase reaction of initial decomposition. And the molten GN affects the precipitous exothermal reaction of FOX-12.","subitem_description_type":"Other"}]},"item_3_description_18":{"attribute_name":"内容記述","attribute_value_mlt":[{"subitem_description":"形態: カラー図版あり","subitem_description_type":"Other"}]},"item_3_description_19":{"attribute_name":"内容記述（英）","attribute_value_mlt":[{"subitem_description":"Physical characteristics: Original contains color illustrations","subitem_description_type":"Other"}]},"item_3_description_32":{"attribute_name":"資料番号","attribute_value_mlt":[{"subitem_description":"資料番号: AA2030016006","subitem_description_type":"Other"}]},"item_3_description_33":{"attribute_name":"レポート番号","attribute_value_mlt":[{"subitem_description":"レポート番号: JAXA-RR-20-007","subitem_description_type":"Other"}]},"item_3_identifier_registration":{"attribute_name":"ID登録","attribute_value_mlt":[{"subitem_identifier_reg_text":"10.20637/00047352","subitem_identifier_reg_type":"JaLC"}]},"item_3_publisher_8":{"attribute_name":"出版者","attribute_value_mlt":[{"subitem_publisher":"宇宙航空研究開発機構(JAXA)"}]},"item_3_publisher_9":{"attribute_name":"出版者（英）","attribute_value_mlt":[{"subitem_publisher":"Japan Aerospace Exploration Agency (JAXA)"}]},"item_3_source_id_22":{"attribute_name":"ISSNONLINE","attribute_value_mlt":[{"subitem_source_identifier":"2433-2216","subitem_source_identifier_type":"ISSN"}]},"item_3_text_6":{"attribute_name":"著者所属","attribute_value_mlt":[{"subitem_text_value":"横浜国立大学"},{"subitem_text_value":"横浜国立大学"},{"subitem_text_value":"横浜国立大学"}]},"item_3_text_7":{"attribute_name":"著者所属（英）","attribute_value_mlt":[{"subitem_text_language":"en","subitem_text_value":"Yokohama National University"},{"subitem_text_language":"en","subitem_text_value":"Yokohama National University"},{"subitem_text_language":"en","subitem_text_value":"Yokohama National University"}]},"item_3_version_type_30":{"attribute_name":"著者版フラグ","attribute_value_mlt":[{"subitem_version_resource":"http://purl.org/coar/version/c_970fb48d4fbd8a85","subitem_version_type":"VoR"}]},"item_creator":{"attribute_name":"著者","attribute_type":"creator","attribute_value_mlt":[{"creatorNames":[{"creatorName":"塩田, 謙人"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"伊里, 友一朗"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"三宅, 淳巳"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"SHIOTA, Kento","creatorNameLang":"en"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"IZATO, Yuichiro","creatorNameLang":"en"}],"nameIdentifiers":[{}]},{"creatorNames":[{"creatorName":"MIYAKE, Atsumi","creatorNameLang":"en"}],"nameIdentifiers":[{}]}]},"item_files":{"attribute_name":"ファイル情報","attribute_type":"file","attribute_value_mlt":[{"accessrole":"open_date","date":[{"dateType":"Available","dateValue":"2021-02-10"}],"displaytype":"detail","filename":"AA2030016006.pdf","filesize":[{"value":"4.2 MB"}],"format":"application/pdf","licensetype":"license_note","mimetype":"application/pdf","url":{"label":"AA2030016006.pdf","url":"https://jaxa.repo.nii.ac.jp/record/47365/files/AA2030016006.pdf"},"version_id":"d33333ef-598f-4b56-89f0-67721eefe700"}]},"item_keyword":{"attribute_name":"キーワード","attribute_value_mlt":[{"subitem_subject":"FOX-12","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Decomposition","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Differential Scanning Calorimetry","subitem_subject_language":"en","subitem_subject_scheme":"Other"},{"subitem_subject":"Raman Spectrometry","subitem_subject_language":"en","subitem_subject_scheme":"Other"}]},"item_language":{"attribute_name":"言語","attribute_value_mlt":[{"subitem_language":"jpn"}]},"item_resource_type":{"attribute_name":"資源タイプ","attribute_value_mlt":[{"resourcetype":"technical report","resourceuri":"http://purl.org/coar/resource_type/c_18gh"}]},"item_title":"熱分析とその場観察および分光分析に基づくFOX-12の熱分解特性解析","item_titles":{"attribute_name":"タイトル","attribute_value_mlt":[{"subitem_title":"熱分析とその場観察および分光分析に基づくFOX-12の熱分解特性解析"}]},"item_type_id":"3","owner":"1","path":["1893","2113","2114"],"pubdate":{"attribute_name":"公開日","attribute_value":"2021-02-10"},"publish_date":"2021-02-10","publish_status":"0","recid":"47365","relation_version_is_last":true,"title":["熱分析とその場観察および分光分析に基づくFOX-12の熱分解特性解析"],"weko_creator_id":"1","weko_shared_id":1},"updated":"2023-06-20T19:40:16.517901+00:00"}