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熱分析とその場観察および分光分析に基づくFOX-12の熱分解特性解析
https://doi.org/10.20637/00047352
https://doi.org/10.20637/000473529a717d60-aa84-43f8-a8b9-b62bb19aa3a3
名前 / ファイル | ライセンス | アクション |
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AA2030016006.pdf (4.2 MB)
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Item type | テクニカルレポート / Technical Report(1) | |||||
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公開日 | 2021-02-10 | |||||
タイトル | ||||||
タイトル | 熱分析とその場観察および分光分析に基づくFOX-12の熱分解特性解析 | |||||
言語 | ||||||
言語 | jpn | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | FOX-12 | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | Decomposition | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | Differential Scanning Calorimetry | |||||
キーワード | ||||||
言語 | en | |||||
主題Scheme | Other | |||||
主題 | Raman Spectrometry | |||||
資源タイプ | ||||||
資源タイプ識別子 | http://purl.org/coar/resource_type/c_18gh | |||||
資源タイプ | technical report | |||||
ID登録 | ||||||
ID登録 | 10.20637/00047352 | |||||
ID登録タイプ | JaLC | |||||
その他のタイトル(英) | ||||||
その他のタイトル | Study on Thermal Decomposition Characteristic of FOX-12 based on Thermal Analysis with in-situ Observation and Spectroscopic Analysis | |||||
著者 |
塩田, 謙人
× 塩田, 謙人× 伊里, 友一朗× 三宅, 淳巳× SHIOTA, Kento× IZATO, Yuichiro× MIYAKE, Atsumi |
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著者所属 | ||||||
横浜国立大学 | ||||||
著者所属 | ||||||
横浜国立大学 | ||||||
著者所属 | ||||||
横浜国立大学 | ||||||
著者所属(英) | ||||||
en | ||||||
Yokohama National University | ||||||
著者所属(英) | ||||||
en | ||||||
Yokohama National University | ||||||
著者所属(英) | ||||||
en | ||||||
Yokohama National University | ||||||
出版者 | ||||||
出版者 | 宇宙航空研究開発機構(JAXA) | |||||
出版者(英) | ||||||
出版者 | Japan Aerospace Exploration Agency (JAXA) | |||||
書誌情報 |
宇宙航空研究開発機構研究開発報告: 高エネルギー物質研究会: 令和2年度研究成果報告書 en : JAXA Research and Development Report: Technical Report of The Research Activity for High Energy Materials (2020) 巻 JAXA-RR-20-007, p. 22-25, 発行日 2021-02-10 |
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抄録(英) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Guanylurea dinitramide which is usually called FOX-12 is typical dinitramide salts. To obtain better understanding of thermal decomposition characteristic of FOX-12, this paper focused on analysis of initial decomposition of FOX-12 using in situ measurement with differential scanning calorimetry (DSC) and sample observation or Raman spectrometry for understanding decomposition characteristic of FOX-12. We conducted Raman spectroscopic analysis and sample observation during thermal analysis at 1 and 8 C min-1. The experiment results found that thermal behavior of FOX-12 was different by heating rate and formed condensed phase before sharp exotherm at high heating rate. For DSC/Raman result indicated guanidium nitrate (GN) and cyanuric acid formed during thermal decomposition of FOX-12. From observation results, GN and cyanuric acid formed with solid phase reaction of initial decomposition. And the molten GN affects the precipitous exothermal reaction of FOX-12. | |||||
内容記述 | ||||||
内容記述タイプ | Other | |||||
内容記述 | 形態: カラー図版あり | |||||
内容記述(英) | ||||||
内容記述タイプ | Other | |||||
内容記述 | Physical characteristics: Original contains color illustrations | |||||
ISSNONLINE | ||||||
収録物識別子タイプ | ISSN | |||||
収録物識別子 | 2433-2216 | |||||
著者版フラグ | ||||||
出版タイプ | VoR | |||||
出版タイプResource | http://purl.org/coar/version/c_970fb48d4fbd8a85 | |||||
資料番号 | ||||||
内容記述タイプ | Other | |||||
内容記述 | 資料番号: AA2030016006 | |||||
レポート番号 | ||||||
内容記述タイプ | Other | |||||
内容記述 | レポート番号: JAXA-RR-20-007 |